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Table 2 1H-NMR and 13C-NMR of compound 1

From: Isolation, characterization and in vitro anti-salmonellal activity of compounds from stem bark extract of Canarium schweinfurthii

Compound 1 Maniladiol, Quijano et al. [35]
Positions δc
(CD3OD+ CDCl3, 100 MHz)
δH (mult; J)
(CD3OD+ CDCl3, 400 MHz)
δc
(CD3Cl, 125 MHz)
δH (mult; J)
(CD3Cl, 500 MHz)
1 32.9 1.40 (1H;m)
1.12 (1H; m)
38.5 1.64 (1H; m)
0.98 (1H; m)
2 24.5 1.99 (1H; m)
1.52 (1H; m)
27.1 1.62 (1H; m)
1.58 (1H; m)
3 75.4 3.35 (1H;dd; 11.9; 4.8) 78.9 3.22 (1H; dd; 11.5; 4.5)
4 37.1 38.7
5 48.8 1.30 (1H;m) 55.1 0.74 (1H; dd; 11.5; 1.5)
6 18.0 1.45 (1H; m)
1.44 (1H; m)
18.3 1.58 (1H; t; 3.6)
1.41 (1H; dd; 15.5; 12.0)
7 32.4 1.62 (1H; m)
1.38 (1H; m)
32.6 1.54 (1H; t; 3.5)
1.33 (1H; t; 3.6)
8 39.9 39.8
9 46.5 1.06 (1H; m) 46.8 1.51 (1H; dd; 11.0; 6.5)
10 36.6 37.3
11 23.4 1.91 (2H; m) 23.5 1.92 (1H; ddd; 18.5; 11.0; 3.5)
1.86 (1H; ddd; 18.5; 7.0; 4.0)
12 122.3 5.26 (1H; t; 3.4) 122.3 5.25 (1H; t; 3.5)
13 143.7 143.5
14 43.5 43.7
15 34.9 1.71 (1H; m)
1.26 (1H; m)
35.5 1.67 (1H; d; 13.0)
1.31 (1H; dd; 13.0; 5.0)
16 65.0 4.16 (1H; dd; 11.5; 4.9) 66.0 4.20 (1H; dd; 11.5; 5.0)
17 37.0 36.8
18 49.2 2.16 (1H; dd; 11.5; 4.9) 49.0 2.15 (1H; dd; 14.0; 4.5)
19 46.5 1.71 (1H; m)
1.06 (1H; m)
46.5 1.68 (1H; t; 14.0)
1.06 (1H; ddd; 13.5; 4.5; 2.5)
20 30.4 30.9
21 34.0 1.41 (1H; m)
1.13 (1H; m)
34.1 1.36 (1H; t; 3.7)
1.15 (1H; t; 3.6)
22 30.5 1.91 (1H; m)
1.88 (1H; m)
30.5 1.83(1H; t; 3.4)
1.20(1H; t; 3.5)
23 27.8 0.95 (3H; s) 28.0 1.00 (3H; s)
24 21.7 0.86 (3H; s) 15.6 0.79 (3H; s)
25 14.8 0.99 (3H; s) 15.5 0.94 (3H; s)
26 16.24 1.03 (3H; s) 16.8 0.99 (3H; s)
27 26.4 1.27 (3H; s) 27.1 1.22(3H; s)
28 21.4 0.80 (3H; s) 21.4 0.80 (3H; s)
29 32.6 0.90 (3H; s) 33.2 0.89 (3H; s)
30 23.2 0.92 (3H; s) 23.9 0.90 (3H; s)
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