Table 5 13C NMR (100 MHz) data of compounds 4–6
NO. C | Compound 4 CD3OD | Compound 5 CD3OD | Compound 6 CD3OD |
|---|---|---|---|
2 | 155.3 | 157.1 | 162.1 |
3 | 137.3 | 134.2 | 103.0 |
4 | 178.2 | 178.0 | 180.0 |
5 | 161.0 | 161.6 | 164.3 |
6 | 98.2 | 98.5 | 103.1 |
7 | 164.8 | 164.6 | 160.0 |
8 | 93.4 | 94.5 | 98.6 |
9 | 157.4 | 156.6 | 157.0 |
10 | 103.3 | 103.3 | 108.4 |
1’ | 121.3 | 122.2 | 122.4 |
2’ | 115.1 | 116.2 | 129.2 |
3’ | 144.7 | 145.5 | 116.4 |
4’ | 148.4 | 148.4 | 161.6 |
5’ | 115.2 | 116.1 | 116.4 |
6’ | 121.5 | 122.2 | 129.2 |
OCH3 | 58.2 | ||
1” | 101.2 | 103.3 | |
2” | 73.8 | 74.9 | |
3” | 76.8 | 77.3 | |
4” | 72.5 | 72.7 | |
5” | 75.8 | 76.7 | |
6” | 67.1 | 65.9 | |
1″‘ | 102.3 | 102.8 | |
2″‘ | 70.8 | 70.8 | |
3″‘ | 70.0 | 71.2 | |
4″‘ | 71.4 | 71.4 | |
5″‘ | 69.1 | 69.1 | |
6″‘ | 18.1 | 18.2 |