Table 1 LC-MS/MS parameters for quantitation and confirmation
Analyte | Retentiontime (min) | Q1 mass(m/z) | Q3 mass(m/z) | Declustering potential DP(V) | Entrance potential EP(V) | Collision energy CE(V) | Collision cell exit potential CXP(V) |
|---|---|---|---|---|---|---|---|
Isoliquiritigenin | 10.03 | 257.212 | 137.200 | 66 | 10.5 | 27 | 4 |
147.200 | 66 | 10.5 | 25 | 4 | |||
Daidzein | 9.67 | 255.157 | 91.200 | 86 | 11 | 49 | 4 |
65.100 | 86 | 11 | 71 | 4 | |||
Formononetin | 10.13 | 269.215 | 197.200 | 186 | 12 | 45 | 4 |
89.200 | 186 | 12 | 93 | 4 | |||
Dalbergin | 10.12 | 269.164 | 152.000 | 111 | 10.5 | 61 | 4 |
254.000 | 111 | 10.5 | 29 | 10 | |||
Piperidine | 1.27 | 86.175 | 69.100 | 41 | 7.5 | 19 | 4 |
41.000 | 41 | 7.5 | 29 | 4 | |||
Sativanon | 10.21 | 301.262 | 223.000 | 56 | 8.5 | 15 | 4 |
102.400 | 56 | 8.5 | 43 | 4 |